How to obtain good peak shapes and efficiences in liquid chromatography in reversed-phase and hydrophilic interaction separations
(2009)
Presentation / Conference
McCalley, D. V. (2009, June). How to obtain good peak shapes and efficiences in liquid chromatography in reversed-phase and hydrophilic interaction separations. Paper presented at 34th International Symposium on High Performance Liquid Phase Separations, Dresden, Germany
All Outputs (4)
Practical assessment of frictional heating effects and thermostat design on the performance of conventional (3 μm and 5 μm) columns in reversed-phase high-performance liquid chromatography (2009)
Journal Article
Fallas, M. M., Hadley, M. R., & McCalley, D. V. (2009). Practical assessment of frictional heating effects and thermostat design on the performance of conventional (3 μm and 5 μm) columns in reversed-phase high-performance liquid chromatography. Journal of Chromatography A, 1216(18), 3961-3969. https://doi.org/10.1016/j.chroma.2009.03.007A practical investigation of frictional heating effects in conventional C18 columns was undertaken, to investigate whether problems found for sub-2 μm columns were also present for those of particle size 3 μm and 5 μm and different internal diameter.... Read More about Practical assessment of frictional heating effects and thermostat design on the performance of conventional (3 μm and 5 μm) columns in reversed-phase high-performance liquid chromatography.
Some new advantages of HILIC over RP-LC for the separation of drugs and other ionisable compounds (2009)
Presentation / Conference
McCalley, D. V. (2009, April). Some new advantages of HILIC over RP-LC for the separation of drugs and other ionisable compounds. Paper presented at 4th International HILIC Symposium, Haltern, Germany
A new approach to the determination of column overload characteristics in reversed-phase liquid chromatography (2009)
Journal Article
Dai, J., Carr, P. W., & McCalley, D. V. (2009). A new approach to the determination of column overload characteristics in reversed-phase liquid chromatography. Journal of Chromatography A, 1216(12), 2474-2482. https://doi.org/10.1016/j.chroma.2009.01.036Column overloading is very common during the separations of basic analytes in analytical scale reversed-phase liquid chromatography (RPLC). Due to the complex interactions of ionic analytes with stationary and mobile phases, only a very small amount... Read More about A new approach to the determination of column overload characteristics in reversed-phase liquid chromatography.