Skip to main content

Research Repository

Advanced Search

All Outputs (4)

Practical assessment of frictional heating effects and thermostat design on the performance of conventional (3 μm and 5 μm) columns in reversed-phase high-performance liquid chromatography (2009)
Journal Article
Fallas, M. M., Hadley, M. R., & McCalley, D. V. (2009). Practical assessment of frictional heating effects and thermostat design on the performance of conventional (3 μm and 5 μm) columns in reversed-phase high-performance liquid chromatography. Journal of Chromatography A, 1216(18), 3961-3969. https://doi.org/10.1016/j.chroma.2009.03.007

A practical investigation of frictional heating effects in conventional C18 columns was undertaken, to investigate whether problems found for sub-2 μm columns were also present for those of particle size 3 μm and 5 μm and different internal diameter.... Read More about Practical assessment of frictional heating effects and thermostat design on the performance of conventional (3 μm and 5 μm) columns in reversed-phase high-performance liquid chromatography.

A new approach to the determination of column overload characteristics in reversed-phase liquid chromatography (2009)
Journal Article
Dai, J., Carr, P. W., & McCalley, D. V. (2009). A new approach to the determination of column overload characteristics in reversed-phase liquid chromatography. Journal of Chromatography A, 1216(12), 2474-2482. https://doi.org/10.1016/j.chroma.2009.01.036

Column overloading is very common during the separations of basic analytes in analytical scale reversed-phase liquid chromatography (RPLC). Due to the complex interactions of ionic analytes with stationary and mobile phases, only a very small amount... Read More about A new approach to the determination of column overload characteristics in reversed-phase liquid chromatography.